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How To Make Smokeless Powder
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[1> Boil cotton for 30 minutes, in a 2% solution of sodium hydroxide.
[2> Wash the cotton in hot water and allow it to dry.
[3> Mix slowly and carefully at 25 degrees Centigrade, 250 cc. of concentrated
sulfuric acid, 150 cc. of concentrated nitric acid, and 20 cc. of
water. They must be kept at 25 degrees C.
[4> Next place the dried cotton in the acid solution, and stir well with
either a glass or porcelain rod (do not use metal). This should be
done for 35 minutes.
[5> After nitration, the acids are washed away, and the cotton is washed in
boiling water five times, each time for 25 minutes. The cotton is
given several tests with litmus paper. If the litmus test proves
that there is still some acid present, a 2% solution of sodium
bicarbonate should neutralize whatever is left. This is important,
since any remaining acid acts as an impurity to make the explosive
more unstable.
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